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Acid hydrolysis of myo-inositol 1,3,5-orthobenzoate leads regioselectively to 2-O-benzoyl-myo-inositol via a 1,2-bridged 2'-phenyl-1',3'-dioxolan-2'-ylium ion observed by 1H and 13C NMR spectroscopy, providing the precursor for a highly efficient route to the anticancer agent myo-inositol 1,3,4,5,6-pentakisphosphate.

Original publication

DOI

10.1039/b605392k

Type

Journal article

Journal

Chem Commun (Camb)

Publication Date

28/07/2006

Pages

2989 - 2991

Keywords

Acids, Antineoplastic Agents, Hydrolysis, Inositol Phosphates, Magnetic Resonance Spectroscopy, Molecular Conformation, Stereoisomerism